Patent
US 9,460,827PHYSICALLY FUNCTIONALIZED GRAPHENE HYBRID COMPOSITE (GHC) AND ITS APPLICATIONS
Nguyen C. Khe
US
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Patent
Atlas literature
Patent
US 9,460,827Patent drawings and their descriptions. Click a drawing to enlarge it.
FIG. 1 exhibits a Raman spectroscopy chart of graphene, which shows a small G band at approx in ately 1582 c m-4 and a relatively large 2D band (also named "G …
FIG. 2 illustrates a Raman spectroscopy chart of graphene hav in g different layer counts in the structure In the structure hav in g more and more layers, the G …
FIG.3 shows Raman sp ectro s copy for graphite and graphene oxide, grade graphite (top), graphene oxide (n ddle), and reduced graphene oxide (bottom) [39] …
FIG. 4 is a graph 4000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 1 accord in g to an exemplary embod un ent One can reco …
FIG. 5 is a graph 5000 of a Raman spectra f o r an exemplary physically functiona h zed GHC product type 2 accord in g to an exemplary embod un ent One can …
FIG. 6 is a graph 6000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 3 accord in g to an exemplary embod un ent One can see …
FIG. 7 is a transmission electron nc roscope ("TEM ') im age 7000 for an exemplaryphysically functionahzed GHC product type 3 ("GHC₃ ") accord in g to an …
FIG. 8 i s a graph 8000 o f a Raman spectra for an exemplaryphysically functiona h zed GHC product type 5 ("GHC 5 ") accord in g to an exemplary embod n ent …
FIG. 9 is a graph 9000 of a Raman spectra accord in g to an exemplary embod in ent ofphysically functionahzed GHC product type 4 ("GHC4") One can recog ni ze …
FIG. 10 is a color photograph 10000 of a solution of an exemplary physically functionahzed GHC product type 5 or GHC 5 dispersed in isopropanol alcohol ("IPA …
FIG. 11 i s a color photograph 11000 of an exemplary physically functiona h zed GHC product type 4 or GHC₄ powder, accord in g to an exemplary embod im ent …
FIG. 12 is a trans n ssion electron microscope (TEM) in age 12000 for an exemplary physically functiona h zed GHC product type 4 or GHC₄ powder accord in g to …
FIG. 13 is a schematic diagram 13000 of a reactor, which can comprise one or more of the fo llow ing [94] A heat resistant and unoxidized reaction chamber …
FIG. 14 is a table 14000 ofproperties of various exemplary embod un ents of graphene hybrid composites prepared from a first proprietary so li d carbon source …
FIG. 15 is a graph 15000 of X-ray Diffraction ("XRD ") spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embod un ent, [18]
FIG. 16 in dicate XRD for GHC products prepared from different solid carbon sources accord in g to an exemplary embod un ent, carbon source 1 (SGP) and carbon …
FIG. 17 is a graph 17000 of XRD f o r an exemplary GHC product accord in g to an exemplary embod un ent, conta inin g no metal and n nerals (af t er …
FIG. 18 is a graph 18000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry an -SO 3H functional group accord in g to an …
FIG. 19 is a graph 19000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry a CO O H functional group accord ing to an exemplary …
FIG. 20 is a graph 20000 ofoverlayed XRD spectroscopy results for exemplary GHC products accord in g to the exemplary embod im ents; {00034511 DOC } 1200- 011 …
FIG. 21 is a graph20000 of a transmission electron nc roscope ("TEM ") im age for an exemplary GHC product accord in g to an exemplary embod in ent, which …
FIG. 22 is a graph 22000 of TEM im age for exemplary GHC product One can see that both carbon nano tube (lef t) and flakes (right) appeared in the sample …
FIG. 23 is a graph 23000 of Raman spectroscop y results for an exemplary GHC product accord in g to an exemplary embod im ent, [26]
FIG. 24 is a graph 24000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent, [27]
FIG. 25 is a graph 25000 of Raman spectroscopyresults f o r an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with …
FIG. 26 is a graph 26000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent hav in g been subjected to dia zo …
FIG. 27 is a graph 27000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with H 2 …
FIG. 28 is a graph 28000 o f Raman spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embo dim ent, [31]
FIG. 29 is a graph 29000 of Raman spectroscopy f o r an exemplary GHC product accord in g to an exemplary embod im ent [164] The GHC can be functiona h zed by …
FIG. 30 is a flowchart of an exemplary embod im ent of a method 30000 De tailed Description [33] Certa in exemplary embod in ents can provide a graphene hybrid …
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
An electrically conductive element comprising: a physically functionalized graphene hybrid composite (G H C), wherein said physically functionalized G HC: SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.10.750.918.2189.964.svg 0.153 4.797 Chemistry Black and white SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.11.600.1005.2196.1051.svg 0.153 5.32 Chemistry Black and white gpbe e oxide, SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.12.933.1093.1153.1139.svg 0.153 0.733 Chemistry Black and white _ carbon cre a ted via SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.12.1547.1093.1729.1139.svg 0.153 0.607 Chemistry Black and white _ of a c o~ mbinatio -n o f s olid SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.13.600.1180.2105.1226.svg 0.153 5.017 Chemistry Black and white is a powder comprising particles having average diameter less than nanometers; and when analyzed via Raman spectroscopy: shows a major 2D band at approximately 2650 cm -1; shows a minor D and G band at approximately 1350 cm-and approximately 1575 cm⁻¹; and shows an intensity ratio of 2D band over D band and G band greater than 1.
The electrically conductive element of claim 1, wherein: a reactor forming said physically functionalized G H C generates free radicals via at least one of a carbon generator, waste gas exhaustion mechanism, or reaction precursor agitation mechanism.
The electrically conductive element of claim 1, wherein: a carbon generator generates free radicals utilizing a heating element comprising at least one of an infra-red heater, plasma heater, or resistor heater. Page 2 o f 7 PATENT Application 14/047,991 Attorney Docket 1200-011
The electrically conductive element of claim 1, wherein: a reactor manufacturing said physically functionalized GHC is at least one of a vertical, horizontal, round bottom flask, or irregular shape.
The electrically conductive element of claim 1, wherein: said physically functionalized GHC is used with a specific chemical reagent to enhance electrically conductivity as well as chemical and mechanical stability; wherein said specific chemical reagent is a reduction agent; wherein said reduction agent comprises at least one of a metal hydride, NaBH4, hydrazine, NaOH, KOH, Na₂Si 03, sodium, or potassium.
The electrically conductive element of claim 1, wherein: said electrical conductive element comprises at least one of a binder, electrical conductive nano materials comprising nano metals, nano wire, nano rod of metals and semiconductors, nano graphitic carbons comprising fullerene, diamond, carbon nano tube, graphene, or graphite.
The electrically conductive element of claim 1, wherein: said electrical conductive element comprises a binder, wherein said binder is a polymeric binder, glass binder, ceramic binder, or metallic binder.
The electrically conductive element of claim 1, wherein: said electrical conductive element comprises a binder, wherein said binder is a polymeric binder comprises at least one of an electrical conductive polymer, non- conducting polymer, thermos et polymer, cross linking polymer, emulsion polymer, electrolyte or electrolytic polymer, water soluble polymer, or a poly amino acid.
The electrically conductive element of claim 1, wherein: Page 3 of 7 PATENT Application 14/047,991 Attorney Docket 1200-011 said electrical conductive element comprises a binder, wherein said binder comprises at least one of Si 0 2, Ti 0 2, ZnO, M n O, Mn₂O 3, Mn₃ 0 4, A₁₂ O 3, or KCL
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a substantially transparent conductor.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a conductive ink, lacquer, or adhesive.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a highly conductive thi*- film for k tge iete applications such as replacing thi film prepared by vacuum technique for cost reduction.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a conducting powder for energy storage, nano cable, or super capacitor.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by an energy conversion system or a solar cell.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by an electro catalyst.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a biomedical system. Page 4 of 7 PATENT Application 14/047,991 Attorney Docket 1200-011
The electrically conductive element of claim 1, wherein: said electrical conductive element and physically functionalized GHC is comprised by a power generator for a vehicle, said vehicle comprising a lithium battery.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a mechanical strength enhancement composite, or an alloy between said physically
canceled
The electrically conductive element of claim combined with a specific chemical agent in a high element.
The electrically conductive element of claim combined with a specific chemical agent and at comprising ceramic, aerogel, organo clays in a high element. Page 5 of 7 composite, an electro conductive ceramic functionalized GHC with nano metals. 1, wherein: said physically functionalized GHC is mechanical strength electrical conductive 1, wherein: said physically functionalized GHC is least one of binder, reinforced materials mechanical strength electrical conductive
Layer stacks claimed or described, ordered top of device to substrate.
electrically conductive element comprising physically functionalized GHC
Materials described outside the worked examples.
physically functionalized graphene hybrid composite (GHC)
reduction agent
Measurements and analyses referenced in the patent, with their drawing references.
FIG. 1 exhibits a Raman spectroscopy chart of graphene, which shows a small G band at approx in ately 1582 c m-4 and a relatively large 2D band (also named "G …
Performance values and ranges asserted in the specification or claims.
| Property | Value | Material |
|---|---|---|
Raman 2D band position of physically functionalized GHC | 2650 cm⁻¹ | physically functionalized graphene hybrid composite (GHC) |
Related documents with shared materials, methods, properties, or citations.
Patent
Atlas literature
Patent
US 9,460,827Patent drawings and their descriptions. Click a drawing to enlarge it.
FIG. 1 exhibits a Raman spectroscopy chart of graphene, which shows a small G band at approx in ately 1582 c m-4 and a relatively large 2D band (also named "G …
FIG. 2 illustrates a Raman spectroscopy chart of graphene hav in g different layer counts in the structure In the structure hav in g more and more layers, the G …
FIG.3 shows Raman sp ectro s copy for graphite and graphene oxide, grade graphite (top), graphene oxide (n ddle), and reduced graphene oxide (bottom) [39] …
FIG. 4 is a graph 4000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 1 accord in g to an exemplary embod un ent One can reco …
FIG. 5 is a graph 5000 of a Raman spectra f o r an exemplary physically functiona h zed GHC product type 2 accord in g to an exemplary embod un ent One can …
FIG. 6 is a graph 6000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 3 accord in g to an exemplary embod un ent One can see …
FIG. 7 is a transmission electron nc roscope ("TEM ') im age 7000 for an exemplaryphysically functionahzed GHC product type 3 ("GHC₃ ") accord in g to an …
FIG. 8 i s a graph 8000 o f a Raman spectra for an exemplaryphysically functiona h zed GHC product type 5 ("GHC 5 ") accord in g to an exemplary embod n ent …
FIG. 9 is a graph 9000 of a Raman spectra accord in g to an exemplary embod in ent ofphysically functionahzed GHC product type 4 ("GHC4") One can recog ni ze …
FIG. 10 is a color photograph 10000 of a solution of an exemplary physically functionahzed GHC product type 5 or GHC 5 dispersed in isopropanol alcohol ("IPA …
FIG. 11 i s a color photograph 11000 of an exemplary physically functiona h zed GHC product type 4 or GHC₄ powder, accord in g to an exemplary embod im ent …
FIG. 12 is a trans n ssion electron microscope (TEM) in age 12000 for an exemplary physically functiona h zed GHC product type 4 or GHC₄ powder accord in g to …
FIG. 13 is a schematic diagram 13000 of a reactor, which can comprise one or more of the fo llow ing [94] A heat resistant and unoxidized reaction chamber …
FIG. 14 is a table 14000 ofproperties of various exemplary embod un ents of graphene hybrid composites prepared from a first proprietary so li d carbon source …
FIG. 15 is a graph 15000 of X-ray Diffraction ("XRD ") spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embod un ent, [18]
FIG. 16 in dicate XRD for GHC products prepared from different solid carbon sources accord in g to an exemplary embod un ent, carbon source 1 (SGP) and carbon …
FIG. 17 is a graph 17000 of XRD f o r an exemplary GHC product accord in g to an exemplary embod un ent, conta inin g no metal and n nerals (af t er …
FIG. 18 is a graph 18000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry an -SO 3H functional group accord in g to an …
FIG. 19 is a graph 19000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry a CO O H functional group accord ing to an exemplary …
FIG. 20 is a graph 20000 ofoverlayed XRD spectroscopy results for exemplary GHC products accord in g to the exemplary embod im ents; {00034511 DOC } 1200- 011 …
FIG. 21 is a graph20000 of a transmission electron nc roscope ("TEM ") im age for an exemplary GHC product accord in g to an exemplary embod in ent, which …
FIG. 22 is a graph 22000 of TEM im age for exemplary GHC product One can see that both carbon nano tube (lef t) and flakes (right) appeared in the sample …
FIG. 23 is a graph 23000 of Raman spectroscop y results for an exemplary GHC product accord in g to an exemplary embod im ent, [26]
FIG. 24 is a graph 24000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent, [27]
FIG. 25 is a graph 25000 of Raman spectroscopyresults f o r an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with …
FIG. 26 is a graph 26000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent hav in g been subjected to dia zo …
FIG. 27 is a graph 27000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with H 2 …
FIG. 28 is a graph 28000 o f Raman spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embo dim ent, [31]
FIG. 29 is a graph 29000 of Raman spectroscopy f o r an exemplary GHC product accord in g to an exemplary embod im ent [164] The GHC can be functiona h zed by …
FIG. 30 is a flowchart of an exemplary embod im ent of a method 30000 De tailed Description [33] Certa in exemplary embod in ents can provide a graphene hybrid …
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
An electrically conductive element comprising: a physically functionalized graphene hybrid composite (G H C), wherein said physically functionalized G HC: SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.10.750.918.2189.964.svg 0.153 4.797 Chemistry Black and white SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.11.600.1005.2196.1051.svg 0.153 5.32 Chemistry Black and white gpbe e oxide, SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.12.933.1093.1153.1139.svg 0.153 0.733 Chemistry Black and white _ carbon cre a ted via SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.12.1547.1093.1729.1139.svg 0.153 0.607 Chemistry Black and white _ of a c o~ mbinatio -n o f s olid SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.13.600.1180.2105.1226.svg 0.153 5.017 Chemistry Black and white is a powder comprising particles having average diameter less than nanometers; and when analyzed via Raman spectroscopy: shows a major 2D band at approximately 2650 cm -1; shows a minor D and G band at approximately 1350 cm-and approximately 1575 cm⁻¹; and shows an intensity ratio of 2D band over D band and G band greater than 1.
The electrically conductive element of claim 1, wherein: a reactor forming said physically functionalized G H C generates free radicals via at least one of a carbon generator, waste gas exhaustion mechanism, or reaction precursor agitation mechanism.
The electrically conductive element of claim 1, wherein: a carbon generator generates free radicals utilizing a heating element comprising at least one of an infra-red heater, plasma heater, or resistor heater. Page 2 o f 7 PATENT Application 14/047,991 Attorney Docket 1200-011
The electrically conductive element of claim 1, wherein: a reactor manufacturing said physically functionalized GHC is at least one of a vertical, horizontal, round bottom flask, or irregular shape.
The electrically conductive element of claim 1, wherein: said physically functionalized GHC is used with a specific chemical reagent to enhance electrically conductivity as well as chemical and mechanical stability; wherein said specific chemical reagent is a reduction agent; wherein said reduction agent comprises at least one of a metal hydride, NaBH4, hydrazine, NaOH, KOH, Na₂Si 03, sodium, or potassium.
The electrically conductive element of claim 1, wherein: said electrical conductive element comprises at least one of a binder, electrical conductive nano materials comprising nano metals, nano wire, nano rod of metals and semiconductors, nano graphitic carbons comprising fullerene, diamond, carbon nano tube, graphene, or graphite.
The electrically conductive element of claim 1, wherein: said electrical conductive element comprises a binder, wherein said binder is a polymeric binder, glass binder, ceramic binder, or metallic binder.
The electrically conductive element of claim 1, wherein: said electrical conductive element comprises a binder, wherein said binder is a polymeric binder comprises at least one of an electrical conductive polymer, non- conducting polymer, thermos et polymer, cross linking polymer, emulsion polymer, electrolyte or electrolytic polymer, water soluble polymer, or a poly amino acid.
The electrically conductive element of claim 1, wherein: Page 3 of 7 PATENT Application 14/047,991 Attorney Docket 1200-011 said electrical conductive element comprises a binder, wherein said binder comprises at least one of Si 0 2, Ti 0 2, ZnO, M n O, Mn₂O 3, Mn₃ 0 4, A₁₂ O 3, or KCL
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a substantially transparent conductor.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a conductive ink, lacquer, or adhesive.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a highly conductive thi*- film for k tge iete applications such as replacing thi film prepared by vacuum technique for cost reduction.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a conducting powder for energy storage, nano cable, or super capacitor.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by an energy conversion system or a solar cell.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by an electro catalyst.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a biomedical system. Page 4 of 7 PATENT Application 14/047,991 Attorney Docket 1200-011
The electrically conductive element of claim 1, wherein: said electrical conductive element and physically functionalized GHC is comprised by a power generator for a vehicle, said vehicle comprising a lithium battery.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a mechanical strength enhancement composite, or an alloy between said physically
canceled
The electrically conductive element of claim combined with a specific chemical agent in a high element.
The electrically conductive element of claim combined with a specific chemical agent and at comprising ceramic, aerogel, organo clays in a high element. Page 5 of 7 composite, an electro conductive ceramic functionalized GHC with nano metals. 1, wherein: said physically functionalized GHC is mechanical strength electrical conductive 1, wherein: said physically functionalized GHC is least one of binder, reinforced materials mechanical strength electrical conductive
Layer stacks claimed or described, ordered top of device to substrate.
electrically conductive element comprising physically functionalized GHC
Materials described outside the worked examples.
physically functionalized graphene hybrid composite (GHC)
reduction agent
Measurements and analyses referenced in the patent, with their drawing references.
FIG. 1 exhibits a Raman spectroscopy chart of graphene, which shows a small G band at approx in ately 1582 c m-4 and a relatively large 2D band (also named "G …
Performance values and ranges asserted in the specification or claims.
| Property | Value | Material |
|---|---|---|
Raman 2D band position of physically functionalized GHC | 2650 cm⁻¹ | physically functionalized graphene hybrid composite (GHC) |
Related documents with shared materials, methods, properties, or citations.
Patent
Atlas literature
Patent
US 9,460,827Patent drawings and their descriptions. Click a drawing to enlarge it.
FIG. 1 exhibits a Raman spectroscopy chart of graphene, which shows a small G band at approx in ately 1582 c m-4 and a relatively large 2D band (also named "G …
FIG. 2 illustrates a Raman spectroscopy chart of graphene hav in g different layer counts in the structure In the structure hav in g more and more layers, the G …
FIG.3 shows Raman sp ectro s copy for graphite and graphene oxide, grade graphite (top), graphene oxide (n ddle), and reduced graphene oxide (bottom) [39] …
FIG. 4 is a graph 4000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 1 accord in g to an exemplary embod un ent One can reco …
FIG. 5 is a graph 5000 of a Raman spectra f o r an exemplary physically functiona h zed GHC product type 2 accord in g to an exemplary embod un ent One can …
FIG. 6 is a graph 6000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 3 accord in g to an exemplary embod un ent One can see …
FIG. 7 is a transmission electron nc roscope ("TEM ') im age 7000 for an exemplaryphysically functionahzed GHC product type 3 ("GHC₃ ") accord in g to an …
FIG. 8 i s a graph 8000 o f a Raman spectra for an exemplaryphysically functiona h zed GHC product type 5 ("GHC 5 ") accord in g to an exemplary embod n ent …
FIG. 9 is a graph 9000 of a Raman spectra accord in g to an exemplary embod in ent ofphysically functionahzed GHC product type 4 ("GHC4") One can recog ni ze …
FIG. 10 is a color photograph 10000 of a solution of an exemplary physically functionahzed GHC product type 5 or GHC 5 dispersed in isopropanol alcohol ("IPA …
FIG. 11 i s a color photograph 11000 of an exemplary physically functiona h zed GHC product type 4 or GHC₄ powder, accord in g to an exemplary embod im ent …
FIG. 12 is a trans n ssion electron microscope (TEM) in age 12000 for an exemplary physically functiona h zed GHC product type 4 or GHC₄ powder accord in g to …
FIG. 13 is a schematic diagram 13000 of a reactor, which can comprise one or more of the fo llow ing [94] A heat resistant and unoxidized reaction chamber …
FIG. 14 is a table 14000 ofproperties of various exemplary embod un ents of graphene hybrid composites prepared from a first proprietary so li d carbon source …
FIG. 15 is a graph 15000 of X-ray Diffraction ("XRD ") spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embod un ent, [18]
FIG. 16 in dicate XRD for GHC products prepared from different solid carbon sources accord in g to an exemplary embod un ent, carbon source 1 (SGP) and carbon …
FIG. 17 is a graph 17000 of XRD f o r an exemplary GHC product accord in g to an exemplary embod un ent, conta inin g no metal and n nerals (af t er …
FIG. 18 is a graph 18000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry an -SO 3H functional group accord in g to an …
FIG. 19 is a graph 19000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry a CO O H functional group accord ing to an exemplary …
FIG. 20 is a graph 20000 ofoverlayed XRD spectroscopy results for exemplary GHC products accord in g to the exemplary embod im ents; {00034511 DOC } 1200- 011 …
FIG. 21 is a graph20000 of a transmission electron nc roscope ("TEM ") im age for an exemplary GHC product accord in g to an exemplary embod in ent, which …
FIG. 22 is a graph 22000 of TEM im age for exemplary GHC product One can see that both carbon nano tube (lef t) and flakes (right) appeared in the sample …
FIG. 23 is a graph 23000 of Raman spectroscop y results for an exemplary GHC product accord in g to an exemplary embod im ent, [26]
FIG. 24 is a graph 24000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent, [27]
FIG. 25 is a graph 25000 of Raman spectroscopyresults f o r an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with …
FIG. 26 is a graph 26000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent hav in g been subjected to dia zo …
FIG. 27 is a graph 27000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with H 2 …
FIG. 28 is a graph 28000 o f Raman spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embo dim ent, [31]
FIG. 29 is a graph 29000 of Raman spectroscopy f o r an exemplary GHC product accord in g to an exemplary embod im ent [164] The GHC can be functiona h zed by …
FIG. 30 is a flowchart of an exemplary embod im ent of a method 30000 De tailed Description [33] Certa in exemplary embod in ents can provide a graphene hybrid …
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
An electrically conductive element comprising: a physically functionalized graphene hybrid composite (G H C), wherein said physically functionalized G HC: SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.10.750.918.2189.964.svg 0.153 4.797 Chemistry Black and white SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.11.600.1005.2196.1051.svg 0.153 5.32 Chemistry Black and white gpbe e oxide, SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.12.933.1093.1153.1139.svg 0.153 0.733 Chemistry Black and white _ carbon cre a ted via SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.12.1547.1093.1729.1139.svg 0.153 0.607 Chemistry Black and white _ of a c o~ mbinatio -n o f s olid SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.13.600.1180.2105.1226.svg 0.153 5.017 Chemistry Black and white is a powder comprising particles having average diameter less than nanometers; and when analyzed via Raman spectroscopy: shows a major 2D band at approximately 2650 cm -1; shows a minor D and G band at approximately 1350 cm-and approximately 1575 cm⁻¹; and shows an intensity ratio of 2D band over D band and G band greater than 1.
The electrically conductive element of claim 1, wherein: a reactor forming said physically functionalized G H C generates free radicals via at least one of a carbon generator, waste gas exhaustion mechanism, or reaction precursor agitation mechanism.
The electrically conductive element of claim 1, wherein: a carbon generator generates free radicals utilizing a heating element comprising at least one of an infra-red heater, plasma heater, or resistor heater. Page 2 o f 7 PATENT Application 14/047,991 Attorney Docket 1200-011
The electrically conductive element of claim 1, wherein: a reactor manufacturing said physically functionalized GHC is at least one of a vertical, horizontal, round bottom flask, or irregular shape.
The electrically conductive element of claim 1, wherein: said physically functionalized GHC is used with a specific chemical reagent to enhance electrically conductivity as well as chemical and mechanical stability; wherein said specific chemical reagent is a reduction agent; wherein said reduction agent comprises at least one of a metal hydride, NaBH4, hydrazine, NaOH, KOH, Na₂Si 03, sodium, or potassium.
The electrically conductive element of claim 1, wherein: said electrical conductive element comprises at least one of a binder, electrical conductive nano materials comprising nano metals, nano wire, nano rod of metals and semiconductors, nano graphitic carbons comprising fullerene, diamond, carbon nano tube, graphene, or graphite.
The electrically conductive element of claim 1, wherein: said electrical conductive element comprises a binder, wherein said binder is a polymeric binder, glass binder, ceramic binder, or metallic binder.
The electrically conductive element of claim 1, wherein: said electrical conductive element comprises a binder, wherein said binder is a polymeric binder comprises at least one of an electrical conductive polymer, non- conducting polymer, thermos et polymer, cross linking polymer, emulsion polymer, electrolyte or electrolytic polymer, water soluble polymer, or a poly amino acid.
The electrically conductive element of claim 1, wherein: Page 3 of 7 PATENT Application 14/047,991 Attorney Docket 1200-011 said electrical conductive element comprises a binder, wherein said binder comprises at least one of Si 0 2, Ti 0 2, ZnO, M n O, Mn₂O 3, Mn₃ 0 4, A₁₂ O 3, or KCL
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a substantially transparent conductor.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a conductive ink, lacquer, or adhesive.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a highly conductive thi*- film for k tge iete applications such as replacing thi film prepared by vacuum technique for cost reduction.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a conducting powder for energy storage, nano cable, or super capacitor.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by an energy conversion system or a solar cell.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by an electro catalyst.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a biomedical system. Page 4 of 7 PATENT Application 14/047,991 Attorney Docket 1200-011
The electrically conductive element of claim 1, wherein: said electrical conductive element and physically functionalized GHC is comprised by a power generator for a vehicle, said vehicle comprising a lithium battery.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a mechanical strength enhancement composite, or an alloy between said physically
canceled
The electrically conductive element of claim combined with a specific chemical agent in a high element.
The electrically conductive element of claim combined with a specific chemical agent and at comprising ceramic, aerogel, organo clays in a high element. Page 5 of 7 composite, an electro conductive ceramic functionalized GHC with nano metals. 1, wherein: said physically functionalized GHC is mechanical strength electrical conductive 1, wherein: said physically functionalized GHC is least one of binder, reinforced materials mechanical strength electrical conductive
Layer stacks claimed or described, ordered top of device to substrate.
electrically conductive element comprising physically functionalized GHC
Materials described outside the worked examples.
physically functionalized graphene hybrid composite (GHC)
reduction agent
Measurements and analyses referenced in the patent, with their drawing references.
FIG. 1 exhibits a Raman spectroscopy chart of graphene, which shows a small G band at approx in ately 1582 c m-4 and a relatively large 2D band (also named "G …
Performance values and ranges asserted in the specification or claims.
| Property | Value | Material |
|---|---|---|
Raman 2D band position of physically functionalized GHC | 2650 cm⁻¹ | physically functionalized graphene hybrid composite (GHC) |
Related documents with shared materials, methods, properties, or citations.
Patent
Atlas literature
Patent
US 9,460,827Patent drawings and their descriptions. Click a drawing to enlarge it.
FIG. 1 exhibits a Raman spectroscopy chart of graphene, which shows a small G band at approx in ately 1582 c m-4 and a relatively large 2D band (also named "G …
FIG. 2 illustrates a Raman spectroscopy chart of graphene hav in g different layer counts in the structure In the structure hav in g more and more layers, the G …
FIG.3 shows Raman sp ectro s copy for graphite and graphene oxide, grade graphite (top), graphene oxide (n ddle), and reduced graphene oxide (bottom) [39] …
FIG. 4 is a graph 4000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 1 accord in g to an exemplary embod un ent One can reco …
FIG. 5 is a graph 5000 of a Raman spectra f o r an exemplary physically functiona h zed GHC product type 2 accord in g to an exemplary embod un ent One can …
FIG. 6 is a graph 6000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 3 accord in g to an exemplary embod un ent One can see …
FIG. 7 is a transmission electron nc roscope ("TEM ') im age 7000 for an exemplaryphysically functionahzed GHC product type 3 ("GHC₃ ") accord in g to an …
FIG. 8 i s a graph 8000 o f a Raman spectra for an exemplaryphysically functiona h zed GHC product type 5 ("GHC 5 ") accord in g to an exemplary embod n ent …
FIG. 9 is a graph 9000 of a Raman spectra accord in g to an exemplary embod in ent ofphysically functionahzed GHC product type 4 ("GHC4") One can recog ni ze …
FIG. 10 is a color photograph 10000 of a solution of an exemplary physically functionahzed GHC product type 5 or GHC 5 dispersed in isopropanol alcohol ("IPA …
FIG. 11 i s a color photograph 11000 of an exemplary physically functiona h zed GHC product type 4 or GHC₄ powder, accord in g to an exemplary embod im ent …
FIG. 12 is a trans n ssion electron microscope (TEM) in age 12000 for an exemplary physically functiona h zed GHC product type 4 or GHC₄ powder accord in g to …
FIG. 13 is a schematic diagram 13000 of a reactor, which can comprise one or more of the fo llow ing [94] A heat resistant and unoxidized reaction chamber …
FIG. 14 is a table 14000 ofproperties of various exemplary embod un ents of graphene hybrid composites prepared from a first proprietary so li d carbon source …
FIG. 15 is a graph 15000 of X-ray Diffraction ("XRD ") spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embod un ent, [18]
FIG. 16 in dicate XRD for GHC products prepared from different solid carbon sources accord in g to an exemplary embod un ent, carbon source 1 (SGP) and carbon …
FIG. 17 is a graph 17000 of XRD f o r an exemplary GHC product accord in g to an exemplary embod un ent, conta inin g no metal and n nerals (af t er …
FIG. 18 is a graph 18000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry an -SO 3H functional group accord in g to an …
FIG. 19 is a graph 19000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry a CO O H functional group accord ing to an exemplary …
FIG. 20 is a graph 20000 ofoverlayed XRD spectroscopy results for exemplary GHC products accord in g to the exemplary embod im ents; {00034511 DOC } 1200- 011 …
FIG. 21 is a graph20000 of a transmission electron nc roscope ("TEM ") im age for an exemplary GHC product accord in g to an exemplary embod in ent, which …
FIG. 22 is a graph 22000 of TEM im age for exemplary GHC product One can see that both carbon nano tube (lef t) and flakes (right) appeared in the sample …
FIG. 23 is a graph 23000 of Raman spectroscop y results for an exemplary GHC product accord in g to an exemplary embod im ent, [26]
FIG. 24 is a graph 24000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent, [27]
FIG. 25 is a graph 25000 of Raman spectroscopyresults f o r an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with …
FIG. 26 is a graph 26000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent hav in g been subjected to dia zo …
FIG. 27 is a graph 27000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with H 2 …
FIG. 28 is a graph 28000 o f Raman spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embo dim ent, [31]
FIG. 29 is a graph 29000 of Raman spectroscopy f o r an exemplary GHC product accord in g to an exemplary embod im ent [164] The GHC can be functiona h zed by …
FIG. 30 is a flowchart of an exemplary embod im ent of a method 30000 De tailed Description [33] Certa in exemplary embod in ents can provide a graphene hybrid …
Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
An electrically conductive element comprising: a physically functionalized graphene hybrid composite (G H C), wherein said physically functionalized G HC: SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.10.750.918.2189.964.svg 0.153 4.797 Chemistry Black and white SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.11.600.1005.2196.1051.svg 0.153 5.32 Chemistry Black and white gpbe e oxide, SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.12.933.1093.1153.1139.svg 0.153 0.733 Chemistry Black and white _ carbon cre a ted via SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.12.1547.1093.1729.1139.svg 0.153 0.607 Chemistry Black and white _ of a c o~ mbinatio -n o f s olid SVG 14047991.06-01-2016.IOZLKIR₁PXXIFW2.CLM.1.13.600.1180.2105.1226.svg 0.153 5.017 Chemistry Black and white is a powder comprising particles having average diameter less than nanometers; and when analyzed via Raman spectroscopy: shows a major 2D band at approximately 2650 cm -1; shows a minor D and G band at approximately 1350 cm-and approximately 1575 cm⁻¹; and shows an intensity ratio of 2D band over D band and G band greater than 1.
The electrically conductive element of claim 1, wherein: a reactor forming said physically functionalized G H C generates free radicals via at least one of a carbon generator, waste gas exhaustion mechanism, or reaction precursor agitation mechanism.
The electrically conductive element of claim 1, wherein: a carbon generator generates free radicals utilizing a heating element comprising at least one of an infra-red heater, plasma heater, or resistor heater. Page 2 o f 7 PATENT Application 14/047,991 Attorney Docket 1200-011
The electrically conductive element of claim 1, wherein: a reactor manufacturing said physically functionalized GHC is at least one of a vertical, horizontal, round bottom flask, or irregular shape.
The electrically conductive element of claim 1, wherein: said physically functionalized GHC is used with a specific chemical reagent to enhance electrically conductivity as well as chemical and mechanical stability; wherein said specific chemical reagent is a reduction agent; wherein said reduction agent comprises at least one of a metal hydride, NaBH4, hydrazine, NaOH, KOH, Na₂Si 03, sodium, or potassium.
The electrically conductive element of claim 1, wherein: said electrical conductive element comprises at least one of a binder, electrical conductive nano materials comprising nano metals, nano wire, nano rod of metals and semiconductors, nano graphitic carbons comprising fullerene, diamond, carbon nano tube, graphene, or graphite.
The electrically conductive element of claim 1, wherein: said electrical conductive element comprises a binder, wherein said binder is a polymeric binder, glass binder, ceramic binder, or metallic binder.
The electrically conductive element of claim 1, wherein: said electrical conductive element comprises a binder, wherein said binder is a polymeric binder comprises at least one of an electrical conductive polymer, non- conducting polymer, thermos et polymer, cross linking polymer, emulsion polymer, electrolyte or electrolytic polymer, water soluble polymer, or a poly amino acid.
The electrically conductive element of claim 1, wherein: Page 3 of 7 PATENT Application 14/047,991 Attorney Docket 1200-011 said electrical conductive element comprises a binder, wherein said binder comprises at least one of Si 0 2, Ti 0 2, ZnO, M n O, Mn₂O 3, Mn₃ 0 4, A₁₂ O 3, or KCL
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a substantially transparent conductor.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a conductive ink, lacquer, or adhesive.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a highly conductive thi*- film for k tge iete applications such as replacing thi film prepared by vacuum technique for cost reduction.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a conducting powder for energy storage, nano cable, or super capacitor.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by an energy conversion system or a solar cell.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by an electro catalyst.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a biomedical system. Page 4 of 7 PATENT Application 14/047,991 Attorney Docket 1200-011
The electrically conductive element of claim 1, wherein: said electrical conductive element and physically functionalized GHC is comprised by a power generator for a vehicle, said vehicle comprising a lithium battery.
The electrically conductive element of claim 1, wherein: said electrical conductive element is comprised by a mechanical strength enhancement composite, or an alloy between said physically
canceled
The electrically conductive element of claim combined with a specific chemical agent in a high element.
The electrically conductive element of claim combined with a specific chemical agent and at comprising ceramic, aerogel, organo clays in a high element. Page 5 of 7 composite, an electro conductive ceramic functionalized GHC with nano metals. 1, wherein: said physically functionalized GHC is mechanical strength electrical conductive 1, wherein: said physically functionalized GHC is least one of binder, reinforced materials mechanical strength electrical conductive
Layer stacks claimed or described, ordered top of device to substrate.
electrically conductive element comprising physically functionalized GHC
Materials described outside the worked examples.
physically functionalized graphene hybrid composite (GHC)
reduction agent
Measurements and analyses referenced in the patent, with their drawing references.
FIG. 1 exhibits a Raman spectroscopy chart of graphene, which shows a small G band at approx in ately 1582 c m-4 and a relatively large 2D band (also named "G …
Performance values and ranges asserted in the specification or claims.
| Property | Value | Material |
|---|---|---|
Raman 2D band position of physically functionalized GHC | 2650 cm⁻¹ | physically functionalized graphene hybrid composite (GHC) |
Related documents with shared materials, methods, properties, or citations.
nano graphitic carbons/nano conductive materials
FIG. 2 illustrates a Raman spectroscopy chart of graphene hav in g different layer counts in the structure In the structure hav in g more and more layers, the G …
FIG.3 shows Raman sp ectro s copy for graphite and graphene oxide, grade graphite (top), graphene oxide (n ddle), and reduced graphene oxide (bottom) [39] …
FIG. 4 is a graph 4000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 1 accord in g to an exemplary embod un ent One can reco …
FIG. 5 is a graph 5000 of a Raman spectra f o r an exemplary physically functiona h zed GHC product type 2 accord in g to an exemplary embod un ent One can …
FIG. 6 is a graph 6000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 3 accord in g to an exemplary embod un ent One can see …
FIG. 7 is a transmission electron nc roscope ("TEM ') im age 7000 for an exemplaryphysically functionahzed GHC product type 3 ("GHC₃ ") accord in g to an …
FIG. 8 i s a graph 8000 o f a Raman spectra for an exemplaryphysically functiona h zed GHC product type 5 ("GHC 5 ") accord in g to an exemplary embod n ent …
FIG. 9 is a graph 9000 of a Raman spectra accord in g to an exemplary embod in ent ofphysically functionahzed GHC product type 4 ("GHC4") One can recog ni ze …
FIG. 12 is a trans n ssion electron microscope (TEM) in age 12000 for an exemplary physically functiona h zed GHC product type 4 or GHC₄ powder accord in g to …
FIG. 15 is a graph 15000 of X-ray Diffraction ("XRD ") spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embod un ent, [18]
FIG. 16 in dicate XRD for GHC products prepared from different solid carbon sources accord in g to an exemplary embod un ent, carbon source 1 (SGP) and carbon …
FIG. 17 is a graph 17000 of XRD f o r an exemplary GHC product accord in g to an exemplary embod un ent, conta inin g no metal and n nerals (af t er …
FIG. 18 is a graph 18000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry an -SO 3H functional group accord in g to an …
FIG. 19 is a graph 19000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry a CO O H functional group accord ing to an exemplary …
FIG. 20 is a graph 20000 ofoverlayed XRD spectroscopy results for exemplary GHC products accord in g to the exemplary embod im ents; {00034511 DOC } 1200- 011 …
FIG. 21 is a graph20000 of a transmission electron nc roscope ("TEM ") im age for an exemplary GHC product accord in g to an exemplary embod in ent, which …
FIG. 22 is a graph 22000 of TEM im age for exemplary GHC product One can see that both carbon nano tube (lef t) and flakes (right) appeared in the sample …
FIG. 23 is a graph 23000 of Raman spectroscop y results for an exemplary GHC product accord in g to an exemplary embod im ent, [26]
FIG. 24 is a graph 24000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent, [27]
FIG. 25 is a graph 25000 of Raman spectroscopyresults f o r an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with …
FIG. 26 is a graph 26000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent hav in g been subjected to dia zo …
FIG. 27 is a graph 27000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with H 2 …
FIG. 28 is a graph 28000 o f Raman spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embo dim ent, [31]
FIG. 29 is a graph 29000 of Raman spectroscopy f o r an exemplary GHC product accord in g to an exemplary embod im ent [164] The GHC can be functiona h zed by …
Raman D band position of physically functionalized GHC | 1350 cm⁻¹ | physically functionalized graphene hybrid composite (GHC) |
Raman G band position of physically functionalized GHC | 1575 cm⁻¹ | physically functionalized graphene hybrid composite (GHC) |
Raman intensity ratio I(2D)/(I(D)+I(G)) of physically functionalized GHC | — | physically functionalized graphene hybrid composite (GHC) |
Average particle diameter of physically functionalized GHC powder | — | physically functionalized graphene hybrid composite (GHC) |
Thickness | ≤ 10 nm | — |
PRODUCTION OF GRAPHENE OXIDE
nano graphitic carbons/nano conductive materials
FIG. 2 illustrates a Raman spectroscopy chart of graphene hav in g different layer counts in the structure In the structure hav in g more and more layers, the G …
FIG.3 shows Raman sp ectro s copy for graphite and graphene oxide, grade graphite (top), graphene oxide (n ddle), and reduced graphene oxide (bottom) [39] …
FIG. 4 is a graph 4000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 1 accord in g to an exemplary embod un ent One can reco …
FIG. 5 is a graph 5000 of a Raman spectra f o r an exemplary physically functiona h zed GHC product type 2 accord in g to an exemplary embod un ent One can …
FIG. 6 is a graph 6000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 3 accord in g to an exemplary embod un ent One can see …
FIG. 7 is a transmission electron nc roscope ("TEM ') im age 7000 for an exemplaryphysically functionahzed GHC product type 3 ("GHC₃ ") accord in g to an …
FIG. 8 i s a graph 8000 o f a Raman spectra for an exemplaryphysically functiona h zed GHC product type 5 ("GHC 5 ") accord in g to an exemplary embod n ent …
FIG. 9 is a graph 9000 of a Raman spectra accord in g to an exemplary embod in ent ofphysically functionahzed GHC product type 4 ("GHC4") One can recog ni ze …
FIG. 12 is a trans n ssion electron microscope (TEM) in age 12000 for an exemplary physically functiona h zed GHC product type 4 or GHC₄ powder accord in g to …
FIG. 15 is a graph 15000 of X-ray Diffraction ("XRD ") spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embod un ent, [18]
FIG. 16 in dicate XRD for GHC products prepared from different solid carbon sources accord in g to an exemplary embod un ent, carbon source 1 (SGP) and carbon …
FIG. 17 is a graph 17000 of XRD f o r an exemplary GHC product accord in g to an exemplary embod un ent, conta inin g no metal and n nerals (af t er …
FIG. 18 is a graph 18000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry an -SO 3H functional group accord in g to an …
FIG. 19 is a graph 19000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry a CO O H functional group accord ing to an exemplary …
FIG. 20 is a graph 20000 ofoverlayed XRD spectroscopy results for exemplary GHC products accord in g to the exemplary embod im ents; {00034511 DOC } 1200- 011 …
FIG. 21 is a graph20000 of a transmission electron nc roscope ("TEM ") im age for an exemplary GHC product accord in g to an exemplary embod in ent, which …
FIG. 22 is a graph 22000 of TEM im age for exemplary GHC product One can see that both carbon nano tube (lef t) and flakes (right) appeared in the sample …
FIG. 23 is a graph 23000 of Raman spectroscop y results for an exemplary GHC product accord in g to an exemplary embod im ent, [26]
FIG. 24 is a graph 24000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent, [27]
FIG. 25 is a graph 25000 of Raman spectroscopyresults f o r an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with …
FIG. 26 is a graph 26000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent hav in g been subjected to dia zo …
FIG. 27 is a graph 27000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with H 2 …
FIG. 28 is a graph 28000 o f Raman spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embo dim ent, [31]
FIG. 29 is a graph 29000 of Raman spectroscopy f o r an exemplary GHC product accord in g to an exemplary embod im ent [164] The GHC can be functiona h zed by …
Raman D band position of physically functionalized GHC | 1350 cm⁻¹ | physically functionalized graphene hybrid composite (GHC) |
Raman G band position of physically functionalized GHC | 1575 cm⁻¹ | physically functionalized graphene hybrid composite (GHC) |
Raman intensity ratio I(2D)/(I(D)+I(G)) of physically functionalized GHC | — | physically functionalized graphene hybrid composite (GHC) |
Average particle diameter of physically functionalized GHC powder | — | physically functionalized graphene hybrid composite (GHC) |
Thickness | ≤ 10 nm | — |
PRODUCTION OF GRAPHENE OXIDE
nano graphitic carbons/nano conductive materials
FIG. 2 illustrates a Raman spectroscopy chart of graphene hav in g different layer counts in the structure In the structure hav in g more and more layers, the G …
FIG.3 shows Raman sp ectro s copy for graphite and graphene oxide, grade graphite (top), graphene oxide (n ddle), and reduced graphene oxide (bottom) [39] …
FIG. 4 is a graph 4000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 1 accord in g to an exemplary embod un ent One can reco …
FIG. 5 is a graph 5000 of a Raman spectra f o r an exemplary physically functiona h zed GHC product type 2 accord in g to an exemplary embod un ent One can …
FIG. 6 is a graph 6000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 3 accord in g to an exemplary embod un ent One can see …
FIG. 7 is a transmission electron nc roscope ("TEM ') im age 7000 for an exemplaryphysically functionahzed GHC product type 3 ("GHC₃ ") accord in g to an …
FIG. 8 i s a graph 8000 o f a Raman spectra for an exemplaryphysically functiona h zed GHC product type 5 ("GHC 5 ") accord in g to an exemplary embod n ent …
FIG. 9 is a graph 9000 of a Raman spectra accord in g to an exemplary embod in ent ofphysically functionahzed GHC product type 4 ("GHC4") One can recog ni ze …
FIG. 12 is a trans n ssion electron microscope (TEM) in age 12000 for an exemplary physically functiona h zed GHC product type 4 or GHC₄ powder accord in g to …
FIG. 15 is a graph 15000 of X-ray Diffraction ("XRD ") spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embod un ent, [18]
FIG. 16 in dicate XRD for GHC products prepared from different solid carbon sources accord in g to an exemplary embod un ent, carbon source 1 (SGP) and carbon …
FIG. 17 is a graph 17000 of XRD f o r an exemplary GHC product accord in g to an exemplary embod un ent, conta inin g no metal and n nerals (af t er …
FIG. 18 is a graph 18000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry an -SO 3H functional group accord in g to an …
FIG. 19 is a graph 19000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry a CO O H functional group accord ing to an exemplary …
FIG. 20 is a graph 20000 ofoverlayed XRD spectroscopy results for exemplary GHC products accord in g to the exemplary embod im ents; {00034511 DOC } 1200- 011 …
FIG. 21 is a graph20000 of a transmission electron nc roscope ("TEM ") im age for an exemplary GHC product accord in g to an exemplary embod in ent, which …
FIG. 22 is a graph 22000 of TEM im age for exemplary GHC product One can see that both carbon nano tube (lef t) and flakes (right) appeared in the sample …
FIG. 23 is a graph 23000 of Raman spectroscop y results for an exemplary GHC product accord in g to an exemplary embod im ent, [26]
FIG. 24 is a graph 24000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent, [27]
FIG. 25 is a graph 25000 of Raman spectroscopyresults f o r an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with …
FIG. 26 is a graph 26000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent hav in g been subjected to dia zo …
FIG. 27 is a graph 27000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with H 2 …
FIG. 28 is a graph 28000 o f Raman spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embo dim ent, [31]
FIG. 29 is a graph 29000 of Raman spectroscopy f o r an exemplary GHC product accord in g to an exemplary embod im ent [164] The GHC can be functiona h zed by …
Raman D band position of physically functionalized GHC | 1350 cm⁻¹ | physically functionalized graphene hybrid composite (GHC) |
Raman G band position of physically functionalized GHC | 1575 cm⁻¹ | physically functionalized graphene hybrid composite (GHC) |
Raman intensity ratio I(2D)/(I(D)+I(G)) of physically functionalized GHC | — | physically functionalized graphene hybrid composite (GHC) |
Average particle diameter of physically functionalized GHC powder | — | physically functionalized graphene hybrid composite (GHC) |
Thickness | ≤ 10 nm | — |
PRODUCTION OF GRAPHENE OXIDE
nano graphitic carbons/nano conductive materials
FIG. 2 illustrates a Raman spectroscopy chart of graphene hav in g different layer counts in the structure In the structure hav in g more and more layers, the G …
FIG.3 shows Raman sp ectro s copy for graphite and graphene oxide, grade graphite (top), graphene oxide (n ddle), and reduced graphene oxide (bottom) [39] …
FIG. 4 is a graph 4000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 1 accord in g to an exemplary embod un ent One can reco …
FIG. 5 is a graph 5000 of a Raman spectra f o r an exemplary physically functiona h zed GHC product type 2 accord in g to an exemplary embod un ent One can …
FIG. 6 is a graph 6000 ofa Raman spectra f o r an exemplary physically functiona h zed GHC product type 3 accord in g to an exemplary embod un ent One can see …
FIG. 7 is a transmission electron nc roscope ("TEM ') im age 7000 for an exemplaryphysically functionahzed GHC product type 3 ("GHC₃ ") accord in g to an …
FIG. 8 i s a graph 8000 o f a Raman spectra for an exemplaryphysically functiona h zed GHC product type 5 ("GHC 5 ") accord in g to an exemplary embod n ent …
FIG. 9 is a graph 9000 of a Raman spectra accord in g to an exemplary embod in ent ofphysically functionahzed GHC product type 4 ("GHC4") One can recog ni ze …
FIG. 12 is a trans n ssion electron microscope (TEM) in age 12000 for an exemplary physically functiona h zed GHC product type 4 or GHC₄ powder accord in g to …
FIG. 15 is a graph 15000 of X-ray Diffraction ("XRD ") spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embod un ent, [18]
FIG. 16 in dicate XRD for GHC products prepared from different solid carbon sources accord in g to an exemplary embod un ent, carbon source 1 (SGP) and carbon …
FIG. 17 is a graph 17000 of XRD f o r an exemplary GHC product accord in g to an exemplary embod un ent, conta inin g no metal and n nerals (af t er …
FIG. 18 is a graph 18000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry an -SO 3H functional group accord in g to an …
FIG. 19 is a graph 19000 of XRD spectroscopy results for an exemplary GHC product functiona h zed to carry a CO O H functional group accord ing to an exemplary …
FIG. 20 is a graph 20000 ofoverlayed XRD spectroscopy results for exemplary GHC products accord in g to the exemplary embod im ents; {00034511 DOC } 1200- 011 …
FIG. 21 is a graph20000 of a transmission electron nc roscope ("TEM ") im age for an exemplary GHC product accord in g to an exemplary embod in ent, which …
FIG. 22 is a graph 22000 of TEM im age for exemplary GHC product One can see that both carbon nano tube (lef t) and flakes (right) appeared in the sample …
FIG. 23 is a graph 23000 of Raman spectroscop y results for an exemplary GHC product accord in g to an exemplary embod im ent, [26]
FIG. 24 is a graph 24000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent, [27]
FIG. 25 is a graph 25000 of Raman spectroscopyresults f o r an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with …
FIG. 26 is a graph 26000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod im ent hav in g been subjected to dia zo …
FIG. 27 is a graph 27000 of Raman spectroscopy results for an exemplary GHC product accord in g to an exemplary embod in ent hav in g been oxidized with H 2 …
FIG. 28 is a graph 28000 o f Raman spectroscopy results f o r an exemplary GHC product accord in g to an exemplary embo dim ent, [31]
FIG. 29 is a graph 29000 of Raman spectroscopy f o r an exemplary GHC product accord in g to an exemplary embod im ent [164] The GHC can be functiona h zed by …
Raman D band position of physically functionalized GHC | 1350 cm⁻¹ | physically functionalized graphene hybrid composite (GHC) |
Raman G band position of physically functionalized GHC | 1575 cm⁻¹ | physically functionalized graphene hybrid composite (GHC) |
Raman intensity ratio I(2D)/(I(D)+I(G)) of physically functionalized GHC | — | physically functionalized graphene hybrid composite (GHC) |
Average particle diameter of physically functionalized GHC powder | — | physically functionalized graphene hybrid composite (GHC) |
Thickness | ≤ 10 nm | — |