Patent
US 9,899,671metal oxide precursor
alcohol solvent
FIG. 3 shows a TEM (transmission electron microscopy) image of a metal oxide nanoparticle/graphene composite prepared by Example 1 of the present invention. …
FIG. 4 shows a XRD (X-ray diffraction) graph of a metal oxide nanoparticle/graphene composite prepared by Example 1 and titanium dioxide nanoparticles prepared …
FIG. 4 shows a XRD (X-ray diffraction) graph of a metal oxide nanoparticle/graphene composite prepared by Example 1 and titanium dioxide nanoparticles prepared …
FIG. 5 shows a TGA (thermal gravimetric analysis) graph of metal oxide nanoparticle/graphene composites prepared by Examples 1 to 4 [0043]
FIG. 6 shows a SEM image of titanium dioxide nanoparticles prepared by Comparative Example 1 [0044]
FIG. 7, the C 1 s high-resolution XPS result of the titanium dioxide nanoparticle/graphene composite prepared by Example 1 and the C 1 s high-resolution XPS …
FIG. 8, the result of an HR-TEM analysis 23 conducted on the iron oxide nanoparticle/graphene composite prepared by Example 5 shows that iron oxide …
FIG. 9 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 5 and iron oxide nanoparticles prepared by Comparative Example 3 …
FIG. 9 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 5 and iron oxide nanoparticles prepared by Comparative Example 3 …
FIG. 10 showing the C 1 s high-resolution XPS result of the iron oxide/graphene composite prepared according to Example 5, it was observed that most of the …
FIG. 11 shows a TGA graph of metal oxide nanoparticle/graphene composites prepared by Examples 5 to 8 [0049]
FIG. 12 shows a SEM image of iron oxide nanoparticles prepared by Comparative Example [0050]
FIG. 13, from an SEM analysis result of Example 9, it was observed that tin oxide nanoparticles having a particle size of about 5 to about 30 nm were deposited …
FIG. 14 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 9 and tin oxide nanoparticles prepared by Comparative Example 4 …
FIG. 14 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 9 and tin oxide nanoparticles prepared by Comparative Example 4 …
FIG. 15 showing the C 1 s high-resolution XPS result of the tin oxide/graphene composite prepared according to Example 9, it was observed that most of the …
FIG. 16 shows a TGA graph of a metal oxide nanoparticle/graphene composite prepared by Examples 9 to 11 [0054]
FIG. 17 shows a SEM image of tin oxide nanoparticles prepared by Comparative Example 4 [0055]
FIG. 18, in the case of the titanium dioxide/graphene electrode prepared by Example 12, the discharge capacity of the lithium ions was about 378 mAh/g at a …
FIG. 19a. Furthermore, the charge/discharge property and cyclability of the battery at a high rate was examined while changing the current density from about …
FIG. 20a. Furthermore, the charge/discharge property and 30 cyclability of the battery at a high rate was examined while changing the current density from …
Duration | 10–21600 s | — |
Duration | 60–14400 s | — |
Pressure | 20–600 bar | — |
Pressure | 100–500 bar | — |
Thickness | 1–30 nm | — |
Voltage | 0.01–3 V | — |
Thickness | 5–30 nm | — |
Thickness | 10–20 nm | — |
Thickness | 50–100 nm | — |
Thickness | 10–50 nm | — |
Pressure | ≤ 20 bar | — |
Duration | ≤ 10 seconds | — |
Duration | 0–21600 s | — |
metal oxide precursor
alcohol solvent
FIG. 3 shows a TEM (transmission electron microscopy) image of a metal oxide nanoparticle/graphene composite prepared by Example 1 of the present invention. …
FIG. 4 shows a XRD (X-ray diffraction) graph of a metal oxide nanoparticle/graphene composite prepared by Example 1 and titanium dioxide nanoparticles prepared …
FIG. 4 shows a XRD (X-ray diffraction) graph of a metal oxide nanoparticle/graphene composite prepared by Example 1 and titanium dioxide nanoparticles prepared …
FIG. 5 shows a TGA (thermal gravimetric analysis) graph of metal oxide nanoparticle/graphene composites prepared by Examples 1 to 4 [0043]
FIG. 6 shows a SEM image of titanium dioxide nanoparticles prepared by Comparative Example 1 [0044]
FIG. 7, the C 1 s high-resolution XPS result of the titanium dioxide nanoparticle/graphene composite prepared by Example 1 and the C 1 s high-resolution XPS …
FIG. 8, the result of an HR-TEM analysis 23 conducted on the iron oxide nanoparticle/graphene composite prepared by Example 5 shows that iron oxide …
FIG. 9 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 5 and iron oxide nanoparticles prepared by Comparative Example 3 …
FIG. 9 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 5 and iron oxide nanoparticles prepared by Comparative Example 3 …
FIG. 10 showing the C 1 s high-resolution XPS result of the iron oxide/graphene composite prepared according to Example 5, it was observed that most of the …
FIG. 11 shows a TGA graph of metal oxide nanoparticle/graphene composites prepared by Examples 5 to 8 [0049]
FIG. 12 shows a SEM image of iron oxide nanoparticles prepared by Comparative Example [0050]
FIG. 13, from an SEM analysis result of Example 9, it was observed that tin oxide nanoparticles having a particle size of about 5 to about 30 nm were deposited …
FIG. 14 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 9 and tin oxide nanoparticles prepared by Comparative Example 4 …
FIG. 14 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 9 and tin oxide nanoparticles prepared by Comparative Example 4 …
FIG. 15 showing the C 1 s high-resolution XPS result of the tin oxide/graphene composite prepared according to Example 9, it was observed that most of the …
FIG. 16 shows a TGA graph of a metal oxide nanoparticle/graphene composite prepared by Examples 9 to 11 [0054]
FIG. 17 shows a SEM image of tin oxide nanoparticles prepared by Comparative Example 4 [0055]
FIG. 18, in the case of the titanium dioxide/graphene electrode prepared by Example 12, the discharge capacity of the lithium ions was about 378 mAh/g at a …
FIG. 19a. Furthermore, the charge/discharge property and cyclability of the battery at a high rate was examined while changing the current density from about …
FIG. 20a. Furthermore, the charge/discharge property and 30 cyclability of the battery at a high rate was examined while changing the current density from …
Duration | 10–21600 s | — |
Duration | 60–14400 s | — |
Pressure | 20–600 bar | — |
Pressure | 100–500 bar | — |
Thickness | 1–30 nm | — |
Voltage | 0.01–3 V | — |
Thickness | 5–30 nm | — |
Thickness | 10–20 nm | — |
Thickness | 50–100 nm | — |
Thickness | 10–50 nm | — |
Pressure | ≤ 20 bar | — |
Duration | ≤ 10 seconds | — |
Duration | 0–21600 s | — |
metal oxide precursor
alcohol solvent
FIG. 3 shows a TEM (transmission electron microscopy) image of a metal oxide nanoparticle/graphene composite prepared by Example 1 of the present invention. …
FIG. 4 shows a XRD (X-ray diffraction) graph of a metal oxide nanoparticle/graphene composite prepared by Example 1 and titanium dioxide nanoparticles prepared …
FIG. 4 shows a XRD (X-ray diffraction) graph of a metal oxide nanoparticle/graphene composite prepared by Example 1 and titanium dioxide nanoparticles prepared …
FIG. 5 shows a TGA (thermal gravimetric analysis) graph of metal oxide nanoparticle/graphene composites prepared by Examples 1 to 4 [0043]
FIG. 6 shows a SEM image of titanium dioxide nanoparticles prepared by Comparative Example 1 [0044]
FIG. 7, the C 1 s high-resolution XPS result of the titanium dioxide nanoparticle/graphene composite prepared by Example 1 and the C 1 s high-resolution XPS …
FIG. 8, the result of an HR-TEM analysis 23 conducted on the iron oxide nanoparticle/graphene composite prepared by Example 5 shows that iron oxide …
FIG. 9 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 5 and iron oxide nanoparticles prepared by Comparative Example 3 …
FIG. 9 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 5 and iron oxide nanoparticles prepared by Comparative Example 3 …
FIG. 10 showing the C 1 s high-resolution XPS result of the iron oxide/graphene composite prepared according to Example 5, it was observed that most of the …
FIG. 11 shows a TGA graph of metal oxide nanoparticle/graphene composites prepared by Examples 5 to 8 [0049]
FIG. 12 shows a SEM image of iron oxide nanoparticles prepared by Comparative Example [0050]
FIG. 13, from an SEM analysis result of Example 9, it was observed that tin oxide nanoparticles having a particle size of about 5 to about 30 nm were deposited …
FIG. 14 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 9 and tin oxide nanoparticles prepared by Comparative Example 4 …
FIG. 14 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 9 and tin oxide nanoparticles prepared by Comparative Example 4 …
FIG. 15 showing the C 1 s high-resolution XPS result of the tin oxide/graphene composite prepared according to Example 9, it was observed that most of the …
FIG. 16 shows a TGA graph of a metal oxide nanoparticle/graphene composite prepared by Examples 9 to 11 [0054]
FIG. 17 shows a SEM image of tin oxide nanoparticles prepared by Comparative Example 4 [0055]
FIG. 18, in the case of the titanium dioxide/graphene electrode prepared by Example 12, the discharge capacity of the lithium ions was about 378 mAh/g at a …
FIG. 19a. Furthermore, the charge/discharge property and cyclability of the battery at a high rate was examined while changing the current density from about …
FIG. 20a. Furthermore, the charge/discharge property and 30 cyclability of the battery at a high rate was examined while changing the current density from …
Duration | 10–21600 s | — |
Duration | 60–14400 s | — |
Pressure | 20–600 bar | — |
Pressure | 100–500 bar | — |
Thickness | 1–30 nm | — |
Voltage | 0.01–3 V | — |
Thickness | 5–30 nm | — |
Thickness | 10–20 nm | — |
Thickness | 50–100 nm | — |
Thickness | 10–50 nm | — |
Pressure | ≤ 20 bar | — |
Duration | ≤ 10 seconds | — |
Duration | 0–21600 s | — |
metal oxide precursor
alcohol solvent
FIG. 3 shows a TEM (transmission electron microscopy) image of a metal oxide nanoparticle/graphene composite prepared by Example 1 of the present invention. …
FIG. 4 shows a XRD (X-ray diffraction) graph of a metal oxide nanoparticle/graphene composite prepared by Example 1 and titanium dioxide nanoparticles prepared …
FIG. 4 shows a XRD (X-ray diffraction) graph of a metal oxide nanoparticle/graphene composite prepared by Example 1 and titanium dioxide nanoparticles prepared …
FIG. 5 shows a TGA (thermal gravimetric analysis) graph of metal oxide nanoparticle/graphene composites prepared by Examples 1 to 4 [0043]
FIG. 6 shows a SEM image of titanium dioxide nanoparticles prepared by Comparative Example 1 [0044]
FIG. 7, the C 1 s high-resolution XPS result of the titanium dioxide nanoparticle/graphene composite prepared by Example 1 and the C 1 s high-resolution XPS …
FIG. 8, the result of an HR-TEM analysis 23 conducted on the iron oxide nanoparticle/graphene composite prepared by Example 5 shows that iron oxide …
FIG. 9 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 5 and iron oxide nanoparticles prepared by Comparative Example 3 …
FIG. 9 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 5 and iron oxide nanoparticles prepared by Comparative Example 3 …
FIG. 10 showing the C 1 s high-resolution XPS result of the iron oxide/graphene composite prepared according to Example 5, it was observed that most of the …
FIG. 11 shows a TGA graph of metal oxide nanoparticle/graphene composites prepared by Examples 5 to 8 [0049]
FIG. 12 shows a SEM image of iron oxide nanoparticles prepared by Comparative Example [0050]
FIG. 13, from an SEM analysis result of Example 9, it was observed that tin oxide nanoparticles having a particle size of about 5 to about 30 nm were deposited …
FIG. 14 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 9 and tin oxide nanoparticles prepared by Comparative Example 4 …
FIG. 14 shows a XRD graph of a metal oxide nanoparticle/graphene composite prepared by Example 9 and tin oxide nanoparticles prepared by Comparative Example 4 …
FIG. 15 showing the C 1 s high-resolution XPS result of the tin oxide/graphene composite prepared according to Example 9, it was observed that most of the …
FIG. 16 shows a TGA graph of a metal oxide nanoparticle/graphene composite prepared by Examples 9 to 11 [0054]
FIG. 17 shows a SEM image of tin oxide nanoparticles prepared by Comparative Example 4 [0055]
FIG. 18, in the case of the titanium dioxide/graphene electrode prepared by Example 12, the discharge capacity of the lithium ions was about 378 mAh/g at a …
FIG. 19a. Furthermore, the charge/discharge property and cyclability of the battery at a high rate was examined while changing the current density from about …
FIG. 20a. Furthermore, the charge/discharge property and 30 cyclability of the battery at a high rate was examined while changing the current density from …
Duration | 10–21600 s | — |
Duration | 60–14400 s | — |
Pressure | 20–600 bar | — |
Pressure | 100–500 bar | — |
Thickness | 1–30 nm | — |
Voltage | 0.01–3 V | — |
Thickness | 5–30 nm | — |
Thickness | 10–20 nm | — |
Thickness | 50–100 nm | — |
Thickness | 10–50 nm | — |
Pressure | ≤ 20 bar | — |
Duration | ≤ 10 seconds | — |
Duration | 0–21600 s | — |