Patent
US 9,896,426Patent
Atlas literature
Patent
US 9,896,426Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
(O rigi nal) A met h od for extraction and separation of a flavone component, comp ris ing: modifying graphene to p repared an amination graphene; absorbing and extracting the tlavone component with the amination graphene; wherein the flavone componem is selected from a group comprising -l avones, flavanols, isoflavones, flavanonols, flavanones, anthocyanidins, chalcones and chronones.
(Pre viou sly presented) The method of claim 1 [[211, whewein the amination graphene is an amination graphene-ionic l iquid or an amination g rap henCe -ionic liquid oxide which conpuises a n ionic liquid selected f romv a group comprising 1 -et hyl-3-metyliidazoli tm hexaftluorophosphate, I- ethyl-3- m eth yl imidazoli um bis [(triflu oromet hy l)s td fony Jim ide, 1-bty l-3- meth ylimi daz oli um bis [(trifl u oro methyl) sulfo nyljimide, 1 -buty l -3-met hylinidazolium tetra fl uor ob orate, I -butyl-3- meth yli m idazole c h lo r ide, 1 -buty l-3-m ethyli midazolium bro mide- l-h exylp yridimium trifluoromethanesulfonate, 1 -ethyl- 3-methylim ida z oli um bromide, l.- ethyl -3-methylimidazolium- I odide, I-butyi-3-meth yli ni idazol ium hexatluorophosphate. I- butyl-3 -m ethyli-midazolium bis[(tr i lu oromet hyli)su lfo nyl]im ide, l-ethy l -3-methylim id azol innmte-traf lnoroborate, I,2 -di methy l-3- propyli m idazo ium bis(tri flu oro nrethyl sulfo nyl) imi de, I -ethyl-3-methyl imid azo l ium p- tolenesul fonate, 1 -(cya nomethyl pyridiniurn ch lor ide,.1-hex yllpyridiniumn hex afluorophosphate, I-butr yl-2,3-dimetlylim ida zolium hexafluorophosphate, 1-h exy l -3- methylin idazolitm hexafluorophosphate, trihexyl (te tradecyl)phosphonium hexafluorophosphate, 1 -butyl -_ 2 Applicafion No, 14/948, 248 Docket No,: Y-WK I $ -076-SZWMH-US-076 methylimidazolium c hl ori d e, I-butyl -3-dimetylimidazolium diethyleneglvcolmonomkethylether sulfte, 1b-utyl-3-methylimridoldum r ethanesulfonate, 1-butyl-3~rethyhiidazulium octyl sul f ate, 1 -ami no pyridin ium i odide, 1,2-b is (3-metlylimidazoiium-Ny!) edane dihydroxide, 1 -but yl-3- m eth ylim idaz olium hydro x ide, 1 -methy l-3 -butyli m idazol ium hydroxide, and I- (cya nomethyl)pyridini am chloride.
The method of claim 1, wherein t he flavone component is adsorbed from p l ants; the pla n s comprise een ~Pse&-gink goa c eae., rutaceae, ericaceae, labiatae, umbelliferae, legamtninosae, theaceae meliaceae, com posit e, moraceae and c apri fo liac eae.- & The met h od of claim 7, wherein the plants comp r ise ee*pfes ginkgo leaf, Ro sa roxbunghii, Camellia nitidissima h'l i, black tea, green tea, pu'er tea, dark tea, high mo untain tea, toyeain tea, Ca mel lia sasanqua, sky -itu it, lemon, hawthorn, p omegranate, soybean.
2 -3. C anceled)
(Pre v iously presented) The method of clai m 4, wherein the i onic liquid of the gra phene-basic ionic liquid comprises at least one from I -annopyridinium I odide, I,2-bi s(3- mn ethy limn idazolium -l- yl)et han e dihydroxide, 1 -me thyl-3 -butylim idaz oliuin hydroxide, I~ (cyanometrhyl)pyridini am c h loride, and l -bu tyl -3-m eth yli midazo li um hydroxid&e
6. (Previous ly prese n te d) T h e method of claim 5, wherein the axnina.tion graphene is modified by at least o ne o f ethylenediamine, triethylene tetramine, octadecylamine, dodecylamine, hydrazine hydrate, hydroxylamine, a mm onia, p-chloroaniline, se c- bmtyLin ine, dodecyl-tetr adec yl di methyl amine, n it r oge n amino acid, protein, an d polyamidoamine (PAMA M) dendrimer.
(Previously p r esente d) T he me t hod of claim 8, wherein in the step of adsorbing the flavone 3 Applicat i on No. 14: 948, 248 Docket No,: Y- WK I $- 076-SZ WMH-U--076 co m ponent with ajination wrathenea,diumo atorpon the flavone component is absorbe d fro m lea v es, flowers, fr u its or rhi z omes of the phants 4
Materials described outside the worked examples.
amination graphene
flavone component
Additional fabrication and treatment steps described in the patent.
Patent
Atlas literature
Patent
US 9,896,426Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
(O rigi nal) A met h od for extraction and separation of a flavone component, comp ris ing: modifying graphene to p repared an amination graphene; absorbing and extracting the tlavone component with the amination graphene; wherein the flavone componem is selected from a group comprising -l avones, flavanols, isoflavones, flavanonols, flavanones, anthocyanidins, chalcones and chronones.
(Pre viou sly presented) The method of claim 1 [[211, whewein the amination graphene is an amination graphene-ionic l iquid or an amination g rap henCe -ionic liquid oxide which conpuises a n ionic liquid selected f romv a group comprising 1 -et hyl-3-metyliidazoli tm hexaftluorophosphate, I- ethyl-3- m eth yl imidazoli um bis [(triflu oromet hy l)s td fony Jim ide, 1-bty l-3- meth ylimi daz oli um bis [(trifl u oro methyl) sulfo nyljimide, 1 -buty l -3-met hylinidazolium tetra fl uor ob orate, I -butyl-3- meth yli m idazole c h lo r ide, 1 -buty l-3-m ethyli midazolium bro mide- l-h exylp yridimium trifluoromethanesulfonate, 1 -ethyl- 3-methylim ida z oli um bromide, l.- ethyl -3-methylimidazolium- I odide, I-butyi-3-meth yli ni idazol ium hexatluorophosphate. I- butyl-3 -m ethyli-midazolium bis[(tr i lu oromet hyli)su lfo nyl]im ide, l-ethy l -3-methylim id azol innmte-traf lnoroborate, I,2 -di methy l-3- propyli m idazo ium bis(tri flu oro nrethyl sulfo nyl) imi de, I -ethyl-3-methyl imid azo l ium p- tolenesul fonate, 1 -(cya nomethyl pyridiniurn ch lor ide,.1-hex yllpyridiniumn hex afluorophosphate, I-butr yl-2,3-dimetlylim ida zolium hexafluorophosphate, 1-h exy l -3- methylin idazolitm hexafluorophosphate, trihexyl (te tradecyl)phosphonium hexafluorophosphate, 1 -butyl -_ 2 Applicafion No, 14/948, 248 Docket No,: Y-WK I $ -076-SZWMH-US-076 methylimidazolium c hl ori d e, I-butyl -3-dimetylimidazolium diethyleneglvcolmonomkethylether sulfte, 1b-utyl-3-methylimridoldum r ethanesulfonate, 1-butyl-3~rethyhiidazulium octyl sul f ate, 1 -ami no pyridin ium i odide, 1,2-b is (3-metlylimidazoiium-Ny!) edane dihydroxide, 1 -but yl-3- m eth ylim idaz olium hydro x ide, 1 -methy l-3 -butyli m idazol ium hydroxide, and I- (cya nomethyl)pyridini am chloride.
The method of claim 1, wherein t he flavone component is adsorbed from p l ants; the pla n s comprise een ~Pse&-gink goa c eae., rutaceae, ericaceae, labiatae, umbelliferae, legamtninosae, theaceae meliaceae, com posit e, moraceae and c apri fo liac eae.- & The met h od of claim 7, wherein the plants comp r ise ee*pfes ginkgo leaf, Ro sa roxbunghii, Camellia nitidissima h'l i, black tea, green tea, pu'er tea, dark tea, high mo untain tea, toyeain tea, Ca mel lia sasanqua, sky -itu it, lemon, hawthorn, p omegranate, soybean.
2 -3. C anceled)
(Pre v iously presented) The method of clai m 4, wherein the i onic liquid of the gra phene-basic ionic liquid comprises at least one from I -annopyridinium I odide, I,2-bi s(3- mn ethy limn idazolium -l- yl)et han e dihydroxide, 1 -me thyl-3 -butylim idaz oliuin hydroxide, I~ (cyanometrhyl)pyridini am c h loride, and l -bu tyl -3-m eth yli midazo li um hydroxid&e
6. (Previous ly prese n te d) T h e method of claim 5, wherein the axnina.tion graphene is modified by at least o ne o f ethylenediamine, triethylene tetramine, octadecylamine, dodecylamine, hydrazine hydrate, hydroxylamine, a mm onia, p-chloroaniline, se c- bmtyLin ine, dodecyl-tetr adec yl di methyl amine, n it r oge n amino acid, protein, an d polyamidoamine (PAMA M) dendrimer.
(Previously p r esente d) T he me t hod of claim 8, wherein in the step of adsorbing the flavone 3 Applicat i on No. 14: 948, 248 Docket No,: Y- WK I $- 076-SZ WMH-U--076 co m ponent with ajination wrathenea,diumo atorpon the flavone component is absorbe d fro m lea v es, flowers, fr u its or rhi z omes of the phants 4
Materials described outside the worked examples.
amination graphene
flavone component
Additional fabrication and treatment steps described in the patent.
Patent
Atlas literature
Patent
US 9,896,426Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
(O rigi nal) A met h od for extraction and separation of a flavone component, comp ris ing: modifying graphene to p repared an amination graphene; absorbing and extracting the tlavone component with the amination graphene; wherein the flavone componem is selected from a group comprising -l avones, flavanols, isoflavones, flavanonols, flavanones, anthocyanidins, chalcones and chronones.
(Pre viou sly presented) The method of claim 1 [[211, whewein the amination graphene is an amination graphene-ionic l iquid or an amination g rap henCe -ionic liquid oxide which conpuises a n ionic liquid selected f romv a group comprising 1 -et hyl-3-metyliidazoli tm hexaftluorophosphate, I- ethyl-3- m eth yl imidazoli um bis [(triflu oromet hy l)s td fony Jim ide, 1-bty l-3- meth ylimi daz oli um bis [(trifl u oro methyl) sulfo nyljimide, 1 -buty l -3-met hylinidazolium tetra fl uor ob orate, I -butyl-3- meth yli m idazole c h lo r ide, 1 -buty l-3-m ethyli midazolium bro mide- l-h exylp yridimium trifluoromethanesulfonate, 1 -ethyl- 3-methylim ida z oli um bromide, l.- ethyl -3-methylimidazolium- I odide, I-butyi-3-meth yli ni idazol ium hexatluorophosphate. I- butyl-3 -m ethyli-midazolium bis[(tr i lu oromet hyli)su lfo nyl]im ide, l-ethy l -3-methylim id azol innmte-traf lnoroborate, I,2 -di methy l-3- propyli m idazo ium bis(tri flu oro nrethyl sulfo nyl) imi de, I -ethyl-3-methyl imid azo l ium p- tolenesul fonate, 1 -(cya nomethyl pyridiniurn ch lor ide,.1-hex yllpyridiniumn hex afluorophosphate, I-butr yl-2,3-dimetlylim ida zolium hexafluorophosphate, 1-h exy l -3- methylin idazolitm hexafluorophosphate, trihexyl (te tradecyl)phosphonium hexafluorophosphate, 1 -butyl -_ 2 Applicafion No, 14/948, 248 Docket No,: Y-WK I $ -076-SZWMH-US-076 methylimidazolium c hl ori d e, I-butyl -3-dimetylimidazolium diethyleneglvcolmonomkethylether sulfte, 1b-utyl-3-methylimridoldum r ethanesulfonate, 1-butyl-3~rethyhiidazulium octyl sul f ate, 1 -ami no pyridin ium i odide, 1,2-b is (3-metlylimidazoiium-Ny!) edane dihydroxide, 1 -but yl-3- m eth ylim idaz olium hydro x ide, 1 -methy l-3 -butyli m idazol ium hydroxide, and I- (cya nomethyl)pyridini am chloride.
The method of claim 1, wherein t he flavone component is adsorbed from p l ants; the pla n s comprise een ~Pse&-gink goa c eae., rutaceae, ericaceae, labiatae, umbelliferae, legamtninosae, theaceae meliaceae, com posit e, moraceae and c apri fo liac eae.- & The met h od of claim 7, wherein the plants comp r ise ee*pfes ginkgo leaf, Ro sa roxbunghii, Camellia nitidissima h'l i, black tea, green tea, pu'er tea, dark tea, high mo untain tea, toyeain tea, Ca mel lia sasanqua, sky -itu it, lemon, hawthorn, p omegranate, soybean.
2 -3. C anceled)
(Pre v iously presented) The method of clai m 4, wherein the i onic liquid of the gra phene-basic ionic liquid comprises at least one from I -annopyridinium I odide, I,2-bi s(3- mn ethy limn idazolium -l- yl)et han e dihydroxide, 1 -me thyl-3 -butylim idaz oliuin hydroxide, I~ (cyanometrhyl)pyridini am c h loride, and l -bu tyl -3-m eth yli midazo li um hydroxid&e
6. (Previous ly prese n te d) T h e method of claim 5, wherein the axnina.tion graphene is modified by at least o ne o f ethylenediamine, triethylene tetramine, octadecylamine, dodecylamine, hydrazine hydrate, hydroxylamine, a mm onia, p-chloroaniline, se c- bmtyLin ine, dodecyl-tetr adec yl di methyl amine, n it r oge n amino acid, protein, an d polyamidoamine (PAMA M) dendrimer.
(Previously p r esente d) T he me t hod of claim 8, wherein in the step of adsorbing the flavone 3 Applicat i on No. 14: 948, 248 Docket No,: Y- WK I $- 076-SZ WMH-U--076 co m ponent with ajination wrathenea,diumo atorpon the flavone component is absorbe d fro m lea v es, flowers, fr u its or rhi z omes of the phants 4
Materials described outside the worked examples.
amination graphene
flavone component
Additional fabrication and treatment steps described in the patent.
Patent
Atlas literature
Patent
US 9,896,426Claims define the patent's legal scope. Independent claims stand alone; dependent claims (nested) narrow them. Click a claim to expand its dependents.
(O rigi nal) A met h od for extraction and separation of a flavone component, comp ris ing: modifying graphene to p repared an amination graphene; absorbing and extracting the tlavone component with the amination graphene; wherein the flavone componem is selected from a group comprising -l avones, flavanols, isoflavones, flavanonols, flavanones, anthocyanidins, chalcones and chronones.
(Pre viou sly presented) The method of claim 1 [[211, whewein the amination graphene is an amination graphene-ionic l iquid or an amination g rap henCe -ionic liquid oxide which conpuises a n ionic liquid selected f romv a group comprising 1 -et hyl-3-metyliidazoli tm hexaftluorophosphate, I- ethyl-3- m eth yl imidazoli um bis [(triflu oromet hy l)s td fony Jim ide, 1-bty l-3- meth ylimi daz oli um bis [(trifl u oro methyl) sulfo nyljimide, 1 -buty l -3-met hylinidazolium tetra fl uor ob orate, I -butyl-3- meth yli m idazole c h lo r ide, 1 -buty l-3-m ethyli midazolium bro mide- l-h exylp yridimium trifluoromethanesulfonate, 1 -ethyl- 3-methylim ida z oli um bromide, l.- ethyl -3-methylimidazolium- I odide, I-butyi-3-meth yli ni idazol ium hexatluorophosphate. I- butyl-3 -m ethyli-midazolium bis[(tr i lu oromet hyli)su lfo nyl]im ide, l-ethy l -3-methylim id azol innmte-traf lnoroborate, I,2 -di methy l-3- propyli m idazo ium bis(tri flu oro nrethyl sulfo nyl) imi de, I -ethyl-3-methyl imid azo l ium p- tolenesul fonate, 1 -(cya nomethyl pyridiniurn ch lor ide,.1-hex yllpyridiniumn hex afluorophosphate, I-butr yl-2,3-dimetlylim ida zolium hexafluorophosphate, 1-h exy l -3- methylin idazolitm hexafluorophosphate, trihexyl (te tradecyl)phosphonium hexafluorophosphate, 1 -butyl -_ 2 Applicafion No, 14/948, 248 Docket No,: Y-WK I $ -076-SZWMH-US-076 methylimidazolium c hl ori d e, I-butyl -3-dimetylimidazolium diethyleneglvcolmonomkethylether sulfte, 1b-utyl-3-methylimridoldum r ethanesulfonate, 1-butyl-3~rethyhiidazulium octyl sul f ate, 1 -ami no pyridin ium i odide, 1,2-b is (3-metlylimidazoiium-Ny!) edane dihydroxide, 1 -but yl-3- m eth ylim idaz olium hydro x ide, 1 -methy l-3 -butyli m idazol ium hydroxide, and I- (cya nomethyl)pyridini am chloride.
The method of claim 1, wherein t he flavone component is adsorbed from p l ants; the pla n s comprise een ~Pse&-gink goa c eae., rutaceae, ericaceae, labiatae, umbelliferae, legamtninosae, theaceae meliaceae, com posit e, moraceae and c apri fo liac eae.- & The met h od of claim 7, wherein the plants comp r ise ee*pfes ginkgo leaf, Ro sa roxbunghii, Camellia nitidissima h'l i, black tea, green tea, pu'er tea, dark tea, high mo untain tea, toyeain tea, Ca mel lia sasanqua, sky -itu it, lemon, hawthorn, p omegranate, soybean.
2 -3. C anceled)
(Pre v iously presented) The method of clai m 4, wherein the i onic liquid of the gra phene-basic ionic liquid comprises at least one from I -annopyridinium I odide, I,2-bi s(3- mn ethy limn idazolium -l- yl)et han e dihydroxide, 1 -me thyl-3 -butylim idaz oliuin hydroxide, I~ (cyanometrhyl)pyridini am c h loride, and l -bu tyl -3-m eth yli midazo li um hydroxid&e
6. (Previous ly prese n te d) T h e method of claim 5, wherein the axnina.tion graphene is modified by at least o ne o f ethylenediamine, triethylene tetramine, octadecylamine, dodecylamine, hydrazine hydrate, hydroxylamine, a mm onia, p-chloroaniline, se c- bmtyLin ine, dodecyl-tetr adec yl di methyl amine, n it r oge n amino acid, protein, an d polyamidoamine (PAMA M) dendrimer.
(Previously p r esente d) T he me t hod of claim 8, wherein in the step of adsorbing the flavone 3 Applicat i on No. 14: 948, 248 Docket No,: Y- WK I $- 076-SZ WMH-U--076 co m ponent with ajination wrathenea,diumo atorpon the flavone component is absorbe d fro m lea v es, flowers, fr u its or rhi z omes of the phants 4
Materials described outside the worked examples.
amination graphene
flavone component
Additional fabrication and treatment steps described in the patent.
amination graphene-ionic liquid/amination graphene-ionic liquid oxide
amine modifying agents (ethylenediamine, triethylene tetramine, octadecylamine, dodecylamine, hydrazine hydrate, hydroxylamine, ammonia, p-chloroaniline, sec-butylamine, dodecyl-tetradecyl dimethylamine, nitrogen amino acid, protein, PAMAM dendrimer)
graphene
amination graphene oxide
aminated boron-doped graphene
aminated nitrogen-doped graphene
chitosan-graphene composite membrane
amination graphene-ionic liquid/amination graphene-ionic liquid oxide
amine modifying agents (ethylenediamine, triethylene tetramine, octadecylamine, dodecylamine, hydrazine hydrate, hydroxylamine, ammonia, p-chloroaniline, sec-butylamine, dodecyl-tetradecyl dimethylamine, nitrogen amino acid, protein, PAMAM dendrimer)
graphene
amination graphene oxide
aminated boron-doped graphene
aminated nitrogen-doped graphene
chitosan-graphene composite membrane
amination graphene-ionic liquid/amination graphene-ionic liquid oxide
amine modifying agents (ethylenediamine, triethylene tetramine, octadecylamine, dodecylamine, hydrazine hydrate, hydroxylamine, ammonia, p-chloroaniline, sec-butylamine, dodecyl-tetradecyl dimethylamine, nitrogen amino acid, protein, PAMAM dendrimer)
graphene
amination graphene oxide
aminated boron-doped graphene
aminated nitrogen-doped graphene
chitosan-graphene composite membrane
amination graphene-ionic liquid/amination graphene-ionic liquid oxide
amine modifying agents (ethylenediamine, triethylene tetramine, octadecylamine, dodecylamine, hydrazine hydrate, hydroxylamine, ammonia, p-chloroaniline, sec-butylamine, dodecyl-tetradecyl dimethylamine, nitrogen amino acid, protein, PAMAM dendrimer)
graphene
amination graphene oxide
aminated boron-doped graphene
aminated nitrogen-doped graphene
chitosan-graphene composite membrane
